Properties of Ti-6Al-4V Lattice Structures with In-Situ Alloying and Functional Gradient

Authors

DOI:

https://doi.org/10.20535/2521-1943.2025.9.4(107).339736

Keywords:

lattice structures, Ti-6Al-4V, SLM, LPBF, in-situ alloying, functionally graded materials, mechanical properties, elastic modulus, strength, anisotropy

Abstract

Problem statement. The object of research is lattice structures made of Ti-6Al-4V titanium alloys, manufactured using selective laser melting (SLM) and laser powder bed fusion (LPBF), including in-situ alloyed and functionally graded variants. The problem lies in the lack of systematized data on the relationship between process parameters of additive manufacturing, the resulting microstructure, and mechanical properties, which limits the application of such materials in aerospace industry. Purpose of the study. To determine the influence of in-situ alloying and functional gradient lattice structures on the formation of microstructure, elastic modulus, strength, and energy absorption capacity of Ti-6Al-4V produced by SLM/LPBF. Methodology. Experimental specimens of Ti-6Al-4V–3 % Cr were fabricated by SLM/LPBF under controlled energy density and scanning parameters. The structure was analyzed using X-ray diffraction (XRD), electron microscopy (SEM, EBSD, EDS), and lattice geometry evaluation. In parallel, finite element modelling (FEM) was applied to predict mechanical behavior. Results. The results demonstrate that in-situ alloying with Cr stabilizes the b-phase and controls the distribution of a + b microstructure, thereby increasing alloy strength and stiffness (UTS up to 1050 MPa, elongation 8–10 %). Lattice structures of elliptical and spiral geometry exhibited maximum elastic moduli of 0.76 GPa and 0.41 GPa respectively, while reducing structural mass. Functionally graded lattices with variable strut diameter (1–1.2 mm) ensured more efficient stress transfer and controlled local stiffness. The effect is attributed to substrate preparation and cyclic heating during LPBF, which promoted a¢ martensite decomposition, b-phase stabilization, and stress reduction in critical regions. Conclusions. The novelty of the study lies in the combination of in-situ alloying and functional geometry gradient, which enables achieving an optimal strength-to-weight ratio, improving energy absorption, and providing controlled mechanical response throughout the component volume. Potential applications cover aerospace engineering, where weight reduction under high stiffness and strength is crucial, as well as structural elements with increased resistance to local loading.

References

  1. R. Wauthle et al., “Effects of build orientation and heat treatment on the microstructure and mechanical properties of selective laser melted Ti6Al4V lattice structures,” Additive Manufacturing, Vol. 5, pp. 77–84, 2015, doi: https://doi.org/10.1016/j.addma.2014.12.008.
  2. A. Bandyopadhyay, Y. Zhang, and S. Bose “Recent developments in metal additive manufacturing,” Current Opinion in Chemi-cal Engineering, Vol. 28, 2020, pp. 96–104, doi: https://doi.org/10.1016/j.coche.2020.03.001.
  3. E. Uhlmann et al., “Additive Manufacturing of Titanium Alloy for Aircraft Components”, Procedia CIRP, Vol. 35, pp. 55–60, 2015, doi: https://doi.org/10.1016/j.procir.2015.08.061.
  4. M. Srivastava et al., “Additive manufacturing of Titanium alloy for aerospace applications: Insights into the process, microstruc-ture, and mechanical properties,” Applied Materials Today, Vol. 41, 2024, doi: https://doi.org/10.1016/j.apmt.2024.102481.
  5. X. Yang et al., “Ultra-high specific strength Ti6Al4V alloy lattice material manufactured via selective laser melting,” Materials Science and Engineering: A, Vol. 840, 18, 2022, doi: https://doi.org/10.1016/j.msea.2022.142956.
  6. D. Xu, W. Yang, and P. Cao, “In situ multi-metal alloying in laser-based additive manufacturing: A concise review,” Composites Part B: Engineering, Vol. 299, pp. 112443, 2025, doi: https://doi.org/10.1016/j.compositesb.2025.112443.
  7. C. Chua, S. L. Sing, and C. K. Chua, “Characterisation of in-situ alloyed titanium-tantalum lattice structures by laser powder bed fusion using finite element analysis,” Virtual and Physical Prototyping, Vol. 18, No. 1, pp. 1–13, 2022, doi: https://doi.org/10.1080/17452759.2022.2138463.
  8. S. A. Tyagi and M. Manjaiah, “Additive manufacturing of titanium-based lattice structures for medical applications – A review,” Bioprinting, Vol. 30, 2023, doi: https://doi.org/10.1016/j.bprint.2023.e00267.
  9. V. S. Goettgens et al., “Microstructure and Mechanical Properties of Ti-6Al-4V In Situ Alloyed with 3 wt% Cr by Laser Powder Bed Fusion,” Metals, Vol. 14(6), pp. 715, 2024, doi: https://doi.org/10.3390/met14060715.
  10. W. Xu, E.W. Lui, A. Pateras, M. Qian and M. Brandt, “In situ tailoring microstructure in additively manufactured Ti-6Al-4V for superior mechanical performance,” Acta Mater, vol. 125, pp. 390–400, 2017, doi: https://doi.org/10.1016/j.actamat.2016.12.027.
  11. J. He, D. Li, W. Jiang, L. Ke, G. Qin, Y. Ye, Q. Qin, and D. Qiu, “The Martensitic Transformation and Mechanical Properties of Ti6Al4V Prepared via Selective Laser Melting,” Materials, vol. 12, pp. 321, 2019, doi: https://doi.org/10.3390/ma12020321.
  12. B. Vrancken, L. Thijs, J.P. Kruth, and J. Van Humbeeck, “Heat treatment of Ti6Al4V produced by Selective Laser Melting: Microstructure and mechanical properties,” J. Alloys Compd, vol. 541, pp. 177–185, 2012, doi: https://doi.org/10.1016/j.jallcom.2012.07.022.
  13. V. Cain, L. Thijs, J. Van Humbeeck, B. Van Hooreweder and R. Knutsen, “Crack propagation and fracture toughness of Ti6Al4V alloy produced by selective laser melting,” Addit. Manuf, vol. 5, pp. 68–76, 2015, doi: https://doi.org/10.1016/j.addma.2014.12.006.
  14. H. K. Rafi et al., “Microstructures and mechanical properties of Ti6Al4V parts fabricated by selective laser melting and electron beam melting,” J. Mater. Eng. Perform, Vol. 22, pp. 3872–3883, 2013, doi: 10.1007/s11665-013-0658-0.
  15. L. Facchini et al., “Ductility of a Ti-6Al-4V alloy produced by selective laser melting of prealloyed powders,” Rapid Prototyp. J., Vol. 16, pp. 450–459, 2010, doi: https://doi.org/10.1108/13552541011083371.
  16. T. Vilaro, C. Colin and J. D. Bartout, “As-fabricated and heat-treated microstructures of the Ti-6Al-4V alloy processed by selec-tive laser melting. Metall. Mater. Trans,” A Phys. Metall. Mater. Sci., Vol. 42, pp. 3190–3199, 2011, doi: https://doi.org/10.1007/s11661-011-0731-y.
  17. D. Zhang et al., “Effect of heat treatment on the tensile behavior of selective laser melted Ti-6Al-4V by in situ X-ray characteriza-tion,” Acta Mater., Vol. 189, pp. 93–104, 2020, doi: https://doi.org/10.1016/j.actamat.2020.03.003.
  18. M. H. K. Aljaberi, M. M. Aghdam, T. Goudarzi and M. Al-Waily, “Compressive Behavior of Novel Additively Manufactured Ti-6Al-4V Lattice Structures: Experimental and Numerical Studies,” Materials, Vol. 17(15), 2024, doi: https://doi.org/10.3390/ma17153691.
  19. Santam Engineering and Design, Co. Technical Specifications. Mechanical Engineering Tests. Iran, 2022. Accessed: Jun. 28 2024. [Online]. Available: https://iranlabexpo.ir/resource/links/files/others/36/2/main_eadeed6d2f22c29975d11aba9dd35bbf.pdf.
  20. V. S. Goettgens et al., “Microstructural evolution and mechanical properties of Ti-6Al-4V in situ alloyed with 3.5 wt.% Cu by laser powder bed fusion,” Materialia, Vol. 32, pp. 101928 December 2023, doi: https://doi.org/10.1016/j.mtla.2023.101928.

Published

2025-12-29

How to Cite

[1]
S. Kyrylakha, “Properties of Ti-6Al-4V Lattice Structures with In-Situ Alloying and Functional Gradient”, Mech. Adv. Technol., vol. 9, no. 4(107), pp. 469–482, Dec. 2025.

Issue

Section

Aviation Systems and Technologies